data_0-TOPOS_OXURIK_crb;4/4/t5;sqc184;BCT
_database_code_CSD                  OXURIK
_audit_creation_date                9/7/2021
_audit_creation_method              ToposPro
_chemical_formula_structural        crb;4/4/t5;sqc184;BCT
_chemical_name_systematic
;
catena-(bis(\m-nicotinohydrazide)-bis(\m-nitrato)-methanol-bis(nitrat
o)-di-lead). 
;
_chemical_formula_sum               ZE0
_citation_journal_abbrev            Ultrason.Sonochem.
_citation_year                      2017
_citation_journal_volume            35
_citation_page_first                263
_citation_special_details
;
Experiment details: O6B and O6A disordered over two sites with occupa
ncies 0.52:0.48.. File: O.cif. 
CENTAT: Pb1 Pb2
SIMPLIG: ZA=C6H7N3O
 ZB=CH4O ZC=NO4 ZD=NO3 ZE=Pb
SIMPPAR: METH=Stand; INTRA=V| 
;
loop_
_publ_author_name
'Mirtamizdoust B.'
_cell_length_a                      7.4359
_cell_length_b                      22.4522
_cell_length_c                      14.4797
_cell_angle_alpha                   90
_cell_angle_beta                    93.374
_cell_angle_gamma                   90
_cell_volume                        2413.229
_cell_formula_units_Z               8
_symmetry_space_group_name_H-M      'P 21/c'
_symmetry_Int_Tables_number         14
_refine_ls_R_factor_all             0
loop_
_symmetry_equiv_pos_site_id
_symmetry_equiv_pos_as_xyz
1 x,y,z
2 -x,1/2+y,1/2-z
3 -x,-y,-z
4 x,1/2-y,1/2+z
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_symmetry_multiplicity
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_occupancy
ZE2 ZE 4 0.80230 0.73304 0.55230 1.0000
ZE1 ZE 4 0.23713 0.57993 0.19430 1.0000
loop_
_topol_link.node_label_1
_topol_link.node_label_2
_topol_link.distance
_topol_link.site_symmetry_symop_1
_topol_link.site_symmetry_translation_1_x
_topol_link.site_symmetry_translation_1_y
_topol_link.site_symmetry_translation_1_z
_topol_link.site_symmetry_symop_2
_topol_link.site_symmetry_translation_2_x
_topol_link.site_symmetry_translation_2_y
_topol_link.site_symmetry_translation_2_z
_topol_link.type
_topol_link.multiplicity
ZE2 ZE1 7.9405 1 0 0 0 3 1 1 1 v 4
ZE2 ZE1 7.1494 1 0 0 0 1 1 0 0 v 4
ZE2 ZE1 5.6155 1 0 0 0 4 1 1 0 v 4
ZE2 ZE1 6.3671 1 0 0 0 4 0 1 0 v 4
#End of data_0-TOPOS_OXURIK_crb;4/4/t5;sqc184;BCT