data_0-TOPOS_XATYAV_1,4M8-1
_database_code_CSD                  XATYAV
_audit_creation_date                9/7/2021
_audit_creation_method              ToposPro
_chemical_formula_structural        1,4M8-1
_chemical_name_systematic
;
(1,3-di-t-butyl-4-phenyl-N,N-bis(trimethylsilyl)-1,2-dihydro-1\l^5^,3
,2-diazasilet-2-amine)-dibromo-lead. 
;
_chemical_formula_sum               'ZB0 ZA0 ZC0'
_citation_journal_abbrev            'DALTON TRANS.'
_citation_year                      2017
_citation_journal_volume            46
_citation_page_first                3642
_citation_special_details
;
File: X.cif. 
CENTAT: Pb1
SIMPLIG: ZA=C21H41N3Si3 ZB=Br ZC=Pb
SIMP
PAR: METH=Stand; INTRA=V| 
;
loop_
_publ_author_name
'Yu-Liang SHAN'
'Bi-Xiang LEONG'
'Hong-Wei XI'
'Rakesh GANGULY'
'Yongxin LI'
'Kok HWA LIM'
'Cheuk-Wai SO'
_cell_length_a                      11.043
_cell_length_b                      17.9127
_cell_length_c                      15.2372
_cell_angle_alpha                   90
_cell_angle_beta                    91.423
_cell_angle_gamma                   90
_cell_volume                        3013.14
_cell_formula_units_Z               4
_symmetry_space_group_name_H-M      'P 21/c'
_symmetry_Int_Tables_number         14
_refine_ls_R_factor_all             0
loop_
_symmetry_equiv_pos_site_id
_symmetry_equiv_pos_as_xyz
1 x,y,z
2 -x,1/2+y,1/2-z
3 -x,-y,-z
4 x,1/2-y,1/2+z
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_symmetry_multiplicity
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_occupancy
ZC1 ZC 4 0.85398 0.51300 0.56925 1.0000
ZA1 ZA 4 0.85218 0.34982 0.74046 1.0000
ZB2 ZB 4 0.69459 0.60274 0.65234 1.0000
ZB1 ZB 4 0.05793 0.55931 0.66008 1.0000
loop_
_topol_link.node_label_1
_topol_link.node_label_2
_topol_link.distance
_topol_link.site_symmetry_symop_1
_topol_link.site_symmetry_translation_1_x
_topol_link.site_symmetry_translation_1_y
_topol_link.site_symmetry_translation_1_z
_topol_link.site_symmetry_symop_2
_topol_link.site_symmetry_translation_2_x
_topol_link.site_symmetry_translation_2_y
_topol_link.site_symmetry_translation_2_z
_topol_link.type
_topol_link.multiplicity
ZC1 ZB1 2.7425 1 0 0 0 1 1 0 0 v 4
ZC1 ZB2 2.7195 1 0 0 0 1 0 0 0 v 4
ZC1 ZC1 3.9254 1 0 0 0 3 2 1 1 v 2
ZC1 ZA1 3.9182 1 0 0 0 1 0 0 0 v 4
#End of data_0-TOPOS_XATYAV_1,4M8-1